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Sample Name1VAS
Desired Start P9 GPa
Contents:Sample

Coupler materials

Coupler thickness (µm)

Coupler hole diameter (µm)
1.MgO, KCl, MgFeO (90% Mg, 10% Fe)n/an/a

n/a

Diamonds:Culet diameter(s) & style(s)Cylinder Dia. ThicknessPiston Dia. ThicknessDiamond Types

300 µm2.164 mm1.693 mm1a
Gasket:MaterialInitial Thickness

Regular gasket: hole diameter



Re23 GPa2 DIA = 64.1 µm, 3 DIA = 34.7µm , 4 DIA = 68.6 µm
Cell Configuration:

Downstream Side
i.e. cylinder (default), piston

Downstream Seat
e.g. BA, BN, Slot...

Upstream Seat
e.g. WC std...

Standard Rotation
(mark that is always 'up', e.g. "Cell number on piston".  Slots should always be vertical.)

PistonBAWC stdBlack Arrow
Cell Checks:

Screw Heads  protruding?
(Should be N)

Set screws disengaged?
(Should be Y)

Imperial or Metric Screws?

Offline P Change?
(should be N)

NNMetricN
Current Pressure (GPa):Diffraction Best valueRubyDiamond EdgeSample Raman


11.3 (KCl), 9.1 (MgO), 13.3 (FP)

Photomicrographs:
1) with mark up (or note direction of mark)
2) Include labels, sketch for very complex samplews.

















View(s) from cylinder side (with mark up, or note direction of mark otherwise) INSERT PHOTO OF CELL FROM MICROSCOPE, AND PHOTO OF DAC SHOWING ORIENTATION


View(s) from piston side (with mark up, or note direction of mark otherwise) INSERT PHOTO OF CELL FROM MICROSCOPE, AND PHOTO OF DAC SHOWING ORIENTATION

Interference Fringes
1) note pressure
2) note index of refract.
3) include raw calcs

Chamber
(culet-to-culet)
Downstream Medium(s)

Upstream Medium(s)

Index of Refraction
23.2 umKCl
1.676

XRD Screening













499px

Data

MgFeO, 9 GPa

KCl (white bright), 10 GPa

MgO (4 GPa), KCl and Re contamination everywhere _ this sample is probably not a priority

Grid

Other Information









1VAS

DE KCl

DE MgO

DE FP

d KCl

n KCl

n MgO est.

final

11.3

9.1

13.3

23.21

1.676

1.71


Phase Diagrams







Any Relevant Phase Diagrams & References

Beamline Analysis





Post Mortem

Cell oriented as in XFEL log

Tilt in diamonds visible in scantracker scan #245 (z-scan)


MgFeO grid (25z x 7y) 9GPa
step size: 5um in z, 10um in y

Image Added

Scantracker
#206 #251 (y-scan)
#207 #252 (z-scan)

Image Added




MgO grid (25z 5z x 7y) 15GPa3-4GPa
step size: 5um in z, 10um in y

Image Added

Scantracker
#206 #253 (y-scan)
#207 #254 #255 (z-scan)

Image Added






KCl grid (25z x 7y) 18GPa11GPa
step size: 5um in z, 10um in y
Image Added

Scantracker
#204 #249 (y-scan)
#205 #250 (z-scan)

Image Added